- Product Name 2,5-DIMETHYLBENZONITRILE
- cas 13730-09-1
- purity 99%
Pharmaceutical
Factory Sells Best Quality 2,5-DIMETHYLBENZONITRILE 13730-09-1 with ISO standards
- Molecular Formula: C9H9N
- Molecular Weight: 131.177
- Vapor Pressure: 0.0831mmHg at 25°C
- Melting Point: 13 °C
- Refractive Index: 1.525
- Boiling Point: 226.1 °C at 760 mmHg
- Flash Point: 95.7 °C
- PSA： 23.79000
- Density: 0.99 g/cm3
- LogP: 2.17508
2,5-DIMETHYLBENZONITRILE(Cas 13730-09-1) Usage
|
General Description |
2,5-Dimethylbenzonitrile, also known as 1,6-Dicyan-2,5-hexadiene, is a chemical compound with the molecular formula C9H9N. It is a colorless, clear liquid with a faint odor, and it is commonly used as a reagent in organic synthesis. 2,5-Dimethylbenzonitrile is also used in the production of pharmaceuticals, dyes, and other fine chemicals. While it is not known to be particularly hazardous, exposure to this chemical should be minimized due to its potential to cause irritation to the skin, eyes, and respiratory system. It should be handled with appropriate safety precautions and in a well-ventilated area. |
InChI:InChI=1/C9H9N/c1-7-3-4-8(2)9(5-7)6-10/h3-5H,1-2H3
13730-09-1 Relevant articles
Synergy between heterogeneous catalysis and microwave irradiation in an efficient one-pot synthesis of benzene derivatives via ring-opening of Diels-Alder cycloadducts of substituted furans
De la Hoz,Díaz-Ortiz,Fraile,Gómez,Mayoral,Moreno,Saiz,Vázquez
, p. 753 - 756 (2001)
The use of silica-supported Lewis acids ...
Nitrosation of Cyanamide: Preparation and Properties of the Elusive E- and Z-N'-Cyanodiazohydroxides
Guethner, Thomas,Huber, Evi,Sans, Juergen,Thalhammer, Franz
supporting information, (2020/04/29)
Nitrosation of cyanamide leads to unstab...
Transformation of aromatic bromides into aromatic nitriles with n-BuLi, pivalonitrile, and iodine under metal cyanide-free conditions
Uchida, Ko,Togo, Hideo
, (2019/09/04)
Various aromatic nitriles could be obtai...
Ligand-Promoted Non-Directed C?H Cyanation of Arenes
Liu, Luo-Yan,Yeung, Kap-Sun,Yu, Jin-Quan
supporting information, p. 2199 - 2202 (2019/01/24)
This article reports the first example o...
Sulfuryl Fluoride Mediated Conversion of Aldehydes to Nitriles
Gurjar, Jitendra,Bater, Jorick,Fokin, Valery V.
supporting information, p. 1906 - 1909 (2019/01/24)
Aliphatic, aromatic, and heteroaromatic ...
13730-09-1 Process route
-
-
53957-33-8
2,5-dimethylbenzyl alcohol
-
-
13730-09-1
2,5-dimethylbenzonitrile
Conditions
| Conditions | Yield |
|---|---|
|
2,5-dimethylbenzyl alcohol;
With
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tert-butylhypochlorite;
In
dichloromethane;
at 20 ℃;
for 0.5h;
Inert atmosphere;
With
ammonia; iodine;
In
dichloromethane; water;
at 20 ℃;
for 2h;
Inert atmosphere;
|
99%
|
|
2,5-dimethylbenzyl alcohol;
With
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; iodine;
In
dichloromethane;
at 20 ℃;
for 1h;
With
ammonium hydroxide;
In
dichloromethane;
at 20 ℃;
for 2h;
Reagent/catalyst;
|
99%
|
|
With
ammonium hydroxide; iodine;
at 60 ℃;
for 6h;
|
80%
|
-
-
553-94-6
4-bromo-m-xylene
-
-
68-12-2,33513-42-7
N,N-dimethyl-formamide
-
-
13730-09-1
2,5-dimethylbenzonitrile
Conditions
| Conditions | Yield |
|---|---|
|
4-bromo-m-xylene; N,N-dimethyl-formamide;
With
magnesium;
In
tetrahydrofuran;
at 20 ℃;
With
ammonia; iodine;
In
tetrahydrofuran; water;
at 20 ℃;
|
80%
|
|
4-bromo-m-xylene;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -70 - 0 ℃;
for 0.583333h;
N,N-dimethyl-formamide;
In
tetrahydrofuran; hexane;
at 0 ℃;
for 1h;
With
1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; ammonia;
In
tetrahydrofuran; hexane; water;
at 0 - 20 ℃;
for 2h;
|
64%
|
|
4-bromo-m-xylene;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -70 - 0 ℃;
N,N-dimethyl-formamide;
In
tetrahydrofuran; hexane;
at 0 ℃;
for 1h;
With
ammonia; iodine;
In
tetrahydrofuran; hexane; water;
at 0 - 20 ℃;
|
62%
|
13730-09-1 Upstream products
-
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-
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-
202522-21-2
(2,5-dimethylphenyl)carboaldoxime
-
108-24-7
acetic anhydride
13730-09-1 Downstream products
-
502930-49-6
2,5-dimethyl-α-phenylbenzenemethanimine
-
610-72-0
2,5-dimethylbenzoic acid
-
844-30-4
2,5-Dimethyl-3'-trifluormethyl-benzophenon
-
93-48-1
2,5-dimethylbenzylamine
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