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N,N'-Dimethyl-3,3'-dithiodipropionamide

  • Product Name N,N'-Dimethyl-3,3'-dithiodipropionamide
  • cas 999-72-4
  • purity 99%
Inquiry

N,N'-Dimethyl-3,3'-dithiodipropionamide Good Supplier In Bulk Supply High Purity 999-72-4

  • Molecular Formula: C8H16N2O2S2
  • Molecular Weight: 236.359
  • Melting Point: 111-112 °C 
  • Boiling Point: 510.7 °C at 760 mmHg 
  • PKA: 15.60±0.46(Predicted) 
  • Flash Point: 262.6 °C 
  • PSA: 108.80000 
  • Density: 1.179 g/cm3 
  • LogP: 1.42180 

999-72-4 Relevant articles

One-pot synthesis of 4, 5 - dichloro - 2 - isothiazolinone process

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Paragraph 0036; 0039; 0040, (2017/08/25)

The invention discloses a process for sy...

PREPARATION METHOD OF N,N'-DIALKYL-3,3'-DITHIODIPROPIONAMIDE

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Page/Page column 7, (2013/02/28)

This disclosure relates to a method for ...

Method of preparing N,N′-disubstituted-3,3′-dithiodipropionamide and method of preparing substituted 3-isothiazolone by using the same

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, (2008/06/13)

A method of preparing N,N-disubstituted-...

Nitrosamine-free 3-isothiazolone

-

, (2008/06/13)

Nitrosamine-free 3-isothiazolone biocida...

999-72-4 Process route

dimethyl 3,3'-dithiodipropionate
15441-06-2

dimethyl 3,3'-dithiodipropionate

methylamine
74-89-5

methylamine

N,N'-dimethyl-3,3'-dithiodipropionamide
999-72-4

N,N'-dimethyl-3,3'-dithiodipropionamide

Conditions
Conditions Yield
With sodium sulfite; In water; at 10 ℃; for 24h; Product distribution / selectivity; Inert atmosphere;
97%
With hydrogenchloride;
In methanol; at 5 - 15 ℃; for 24h;
3,3'-dithiobis(propionic acid)
1119-62-6

3,3'-dithiobis(propionic acid)

N,N'-dimethyl-3,3'-dithiodipropionamide
999-72-4

N,N'-dimethyl-3,3'-dithiodipropionamide

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: SOCl2 / benzene / 4 h / Heating
2: CH2 Cl2 / 2 h / Ambient temperature
With thionyl chloride; In dichloromethane; benzene;
Multi-step reaction with 2 steps
1: SOCl2 , Py
With pyridine; thionyl chloride;
Multi-step reaction with 2 steps
1: SOCl2
2: diethyl ether
With thionyl chloride; In diethyl ether;

999-72-4 Upstream products

  • 34631-91-9
    34631-91-9

    2-chloro-5,6-dihydro-[1,3]thiazin-4-one

  • 74-89-5
    74-89-5

    methylamine

  • 15441-06-2
    15441-06-2

    dimethyl 3,3'-dithiodipropionate

  • 1002-18-2
    1002-18-2

    3-(2-chlorocarbonyl-ethyldisulfanyl)-propionyl chloride

999-72-4 Downstream products

  • 26172-55-4
    26172-55-4

    5-chloro-2-methyl-2H-isothiazol-3-one

  • 2682-20-4
    2682-20-4

    2-methyl-3-isothiazolone

  • 26542-23-4
    26542-23-4

    4,5-Dichloro-2-methyl-3(2H)-isothiazolone

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