- Product Name N,N'-Dimethyl-3,3'-dithiodipropionamide
- cas 999-72-4
- purity 99%
N,N'-Dimethyl-3,3'-dithiodipropionamide
N,N'-Dimethyl-3,3'-dithiodipropionamide Good Supplier In Bulk Supply High Purity 999-72-4
- Molecular Formula: C8H16N2O2S2
- Molecular Weight: 236.359
- Melting Point: 111-112 °C
- Boiling Point: 510.7 °C at 760 mmHg
- PKA: 15.60±0.46(Predicted)
- Flash Point: 262.6 °C
- PSA: 108.80000
- Density: 1.179 g/cm3
- LogP: 1.42180
999-72-4 Relevant articles
One-pot synthesis of 4, 5 - dichloro - 2 - isothiazolinone process
-
Paragraph 0036; 0039; 0040, (2017/08/25)
The invention discloses a process for sy...
PREPARATION METHOD OF N,N'-DIALKYL-3,3'-DITHIODIPROPIONAMIDE
-
Page/Page column 7, (2013/02/28)
This disclosure relates to a method for ...
Method of preparing N,N′-disubstituted-3,3′-dithiodipropionamide and method of preparing substituted 3-isothiazolone by using the same
-
, (2008/06/13)
A method of preparing N,N-disubstituted-...
Nitrosamine-free 3-isothiazolone
-
, (2008/06/13)
Nitrosamine-free 3-isothiazolone biocida...
999-72-4 Process route
-
-
15441-06-2
dimethyl 3,3'-dithiodipropionate
-
-
74-89-5
methylamine
-
-
999-72-4
N,N'-dimethyl-3,3'-dithiodipropionamide
| Conditions | Yield |
|---|---|
|
With
sodium sulfite;
In
water;
at 10 ℃;
for 24h;
Product distribution / selectivity;
Inert atmosphere;
|
97%
|
|
With
hydrogenchloride;
|
|
|
In
methanol;
at 5 - 15 ℃;
for 24h;
|
-
-
1119-62-6
3,3'-dithiobis(propionic acid)
-
-
999-72-4
N,N'-dimethyl-3,3'-dithiodipropionamide
| Conditions | Yield |
|---|---|
|
Multi-step reaction
with
2
steps
1: SOCl2
/ benzene / 4 h / Heating
2: CH2
Cl2
/ 2 h / Ambient temperature
With
thionyl chloride;
In
dichloromethane; benzene;
|
|
|
Multi-step reaction
with
2
steps
1: SOCl2
, Py
With
pyridine; thionyl chloride;
|
|
|
Multi-step reaction
with
2
steps
1: SOCl2
2: diethyl ether
With
thionyl chloride;
In
diethyl ether;
|
999-72-4 Upstream products
-
34631-91-9
2-chloro-5,6-dihydro-[1,3]thiazin-4-one
-
74-89-5
methylamine
-
15441-06-2
dimethyl 3,3'-dithiodipropionate
-
1002-18-2
3-(2-chlorocarbonyl-ethyldisulfanyl)-propionyl chloride
999-72-4 Downstream products
-
26172-55-4
5-chloro-2-methyl-2H-isothiazol-3-one
-
2682-20-4
2-methyl-3-isothiazolone
-
26542-23-4
4,5-Dichloro-2-methyl-3(2H)-isothiazolone